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Course, academic year 2023/2024
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Laboratory Technique Advanced - MC240C22E
Title: Laboratorní technika (a)
Guaranteed by: Department of Inorganic Chemistry (31-240)
Faculty: Faculty of Science
Actual: from 2018
Semester: both
E-Credits: 6
Hours per week, examination: 0/4, C [HT]
Capacity: unlimited
Min. number of students: unlimited
4EU+: no
Virtual mobility / capacity: no
State of the course: cancelled
Language: English
Is provided by: MC240C22
Additional information: http://dl2.cuni.cz/course/view.php?id=1816
Note: enabled for web enrollment
you can enroll for the course in winter and in summer semester
Guarantor: prof. RNDr. Jan Kotek, Ph.D.
Incompatibility : MC240C22, MC240C24, MC240C39, MC240C40, MC240C40E, MC250C01, MC250C01N
Is incompatible with: MC240C40E, MC250C01, MC250C01N
Opinion survey results   Examination dates   Schedule   
Annotation -
Last update: doc. RNDr. Vojtěch Kubíček, Ph.D. (03.05.2011)
This course covers basic laboratory training and is designed for students of "Chemistry in Science", "Teaching of Chemistry", and "Biology". The training proceeds during winter semester and the subject is endowed by 6 credits. The subject is identical with C240C40; only difference is that the training of this course proceeds during summer semester. The course puts the laboratory experience of the students gained at secondary school to an equal level and gets them ready for all following laboratory trainings. After absolving of the course, the students have the basic skills including handling the most frequently used laboratory equipments (pH-meter, UV-Vis spectrophotometer, vacuum rotary evaporator) and have the necessary information about safety rules as well as about writing laboratory diaries. The training is organized in blocks of four hours a week. The students work in groups of two according to a firm schedule so that each group absolve the complete set of (all) 10 exercises during semester. In the exercises, measurements of properties of unknown samples, basic synthetic and purification operations and basic methods of analyses are involved.
Literature - Czech
Last update: doc. RNDr. Vojtěch Kubíček, Ph.D. (03.05.2011)

Jan Kotek: Laboratorní technika, Univerzita Karlova v Praze, nakladatelství Karolinum, Praha 2007

Requirements to the exam -
Last update: prof. RNDr. Jan Kotek, Ph.D. (06.12.2011)

Students have to finish all laboratory works, write all protocols and pass a final examination test.

Syllabus -
Last update: doc. RNDr. Vojtěch Kubíček, Ph.D. (07.10.2013)

List of exercises:


  1. Preparation of glycine

  2. Determination of dissociation constant of acetic acid

  3. Electrolytic preparation and electrogravimetry

  4. Preparation of complexes I

  5. Preparation of complexes II

  6. Preparation of pentyl acetate

  7. Determination of distribution coefficient of iodine

  8. Preparation of colour pigments

  9. Rectification and gas handling

  10. Spectrophotometric determination of solubility product


Entry requirements -
Last update: doc. RNDr. Vojtěch Kubíček, Ph.D. (07.10.2013)

Students have to pass a test before entering the course.

 
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