Chemistry Laboratory - MC260C66

• Anglický název: Chemistry Laboratory
• Zajišťuje: Katedra fyzikální a makromol. chemie (31-260)
• Fakulta: Přírodovědecká fakulta
• Platnost: od 2025
• Semestr: letní
• E-Kredity: 5
• Způsob provedení zkoušky: letní s.:
• Rozsah, examinace: letní s.:0/4, Z [HT]
• Počet míst: neomezen
• Minimální obsazenost: neomezen
• 4EU+: ne
• Virtuální mobilita / počet míst pro virtuální mobilitu: ne
• Stav předmětu: vyučován
• Jazyk výuky: angličtina
• Poznámka: povolen pro zápis po webu; při zápisu přednost, je-li ve stud. plánu
• Garant: Mgr. Pavla Eliášová, Ph.D.
• Vyučující: prof. Ing. Jiří Čejka, DrSc.; Mgr. Pavla Eliášová, Ph.D.; Mgr. et Mgr. Martin Kamlar, Ph.D.; Ing. Jan Přech, Ph.D.; doc. RNDr. Ondřej Sedláček, Ph.D.; prof. RNDr. Jan Veselý, Ph.D.

Anotace

The course Chemistry Laboratory aims to provide a general introduction to
the practical aspects of methods in chemical laboratory.
The students should get a knowledge on basis of organic and inorganic synthesis including crystallization,
distillation, or pH measurement. Introduction to diffraction methods, microscopy, spectroscopy, nuclear magnetic
resonance, separation methods including chromatography, and electrochemical methods will be provided.

Poslední úprava: Ušelová Kateřina, RNDr., Ph.D. (07.02.2022)

Literatura

J. Lynch – Physico-Chemical Analysis of Industrial Catalysts, TECHNIP 2003 J.W. Niemantsverdriet – Spectroscopy in Catalysis, VCH 1993 C. Giacovazzo - Fundamentals of Crystallography, Oxford University Press 2011 T.D. Claridge: High-resolution NMR Techniques in Organic Chemistry, Elsevier, 2009 D.B. Williams, C.B. Carter - Transmission Electron Microscopy - A Textbook for Materials Science, 2009 J.M. Thompson – Infrared Spectroscopy, Taylor and Francis 2018

Poslední úprava: Ušelová Kateřina, RNDr., Ph.D. (26.05.2022)

Požadavky ke zkoušce

100 % participation in laboratory. Successful passing of two tests. Acceptance of laboratory reports.

Poslední úprava: Ušelová Kateřina, RNDr., Ph.D. (02.02.2022)

Sylabus

• Introduction. Goals of studies. Good laboratory practice. Safety in laboratory. Basic principles of inorganic synthesis - filtration, centrifugation, pH measurement

• Basic principles of inorganic synthesis - crystallization, preparation of a crystal material, autoclaves, X-ray diffraction

• Basic principles of organic synthesis - crystallization, distillation, determination of melting points

• Basic principles of organic synthesis - preparation of compounds, which will be characterized by different methods

• Synthesis of golden nanoparticles and their characterization by TEM

• Characterization of golden nanoparticles in solution (hydrodynamic radius, electrophoretic mobility) by ZetaSizer and UV-Vis spectroscopy

• Basic principles of organic synthesis - column separation of natural compounds

• Calorimetry

• Liquid NMR - measurement and determination of structure of compounds prepared ad 4) and 6)

• FTIR Spectroscopy - preparation of samples - KBr, self-supporting wafers methods, determination of acidity of sample prepared ad 2)

• Catalytic experiment - samples prepared ad 2) quick experiment in a liquid phase followed by gas chromatography and GC/MS

• Electrochemical methods - Potentiometry, Voltammetry

Poslední úprava: Ušelová Kateřina, RNDr., Ph.D. (02.02.2022)