Analytical Spectrometry - MC230P81

• Anglický název: Analytical Spectrometry
• Český název: Analytická Spektrometrie
• Zajišťuje: Katedra analytické chemie (31-230)
• Fakulta: Přírodovědecká fakulta
• Platnost: od 2023
• Semestr: zimní
• E-Kredity: 2
• Způsob provedení zkoušky: zimní s.:kombinovaná
• Rozsah, examinace: zimní s.:2/0, Zk [HT]
• Počet míst: neomezen
• Minimální obsazenost: neomezen
• 4EU+: ne
• Virtuální mobilita / počet míst pro virtuální mobilitu: ne
• Stav předmětu: vyučován
• Jazyk výuky: angličtina
• Poznámka: povolen pro zápis po webu
• Garant: RNDr. Jakub Hraníček, Ph.D.
• Vyučující: RNDr. Jakub Hraníček, Ph.D.; RNDr. Jan Kratzer, Ph.D.; RNDr. Eliška Nováková, Ph.D.

Anotace

This course is taught in English for Erasmus students and is a basic introduction to the spectrometric methods useful in analytical chemistry. Lectures presented in English contain basic information about the following areas: X-ray spectrometry, atomic absorption, and emission techniques, molecular absorption in UV, VIS, and IR regions, molecular fluorescence, and nuclear magnetic resonance. Individual topics are briefly characterized in the syllabus. All topics are completed with theoretical principles, instrumentation, and practical utilization, mainly in analytical chemistry.

Speakers:
RNDr. Jakub Hraníček, Ph.D.; [e-mail]
RNDr. Jan Kratzer, Ph.D.; [e-mail]
RNDr. Eliška Nováková, Ph.D.: [e-mail]

Academic year 2024/2025
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Tuesday, 09:50 a.m. in the library of the Department of Analytical Chemistry (no. 117).


Program:

8.10. Information meeting, organization, Introduction to the Analytical Spectrometry (JH)

15.10. UV-VIS Spectrometry (EN)

22.10. Infrared Spectrometry (JH)

29.10. Molecular Fluorescence Spectrometry + methods based on the radiation scattering (EN)

5.11. Atomic Absorption Spectrometry (JK)

12.11. Atomic Emission and Fluorescence Spectrometry (JK)

19.11. Inductively Coupled Plasma Mass Spectrometry + approaches to sample treatment (JK)
(Excursion to the Institute of Analytical Chemistry of the CAS, v. v. i.)

26.11. Nuclear Magnetic Resonance Spectrometry (EN)

3.12. X-ray Spectrometry (JH)

10.12. Student´s presentation (JH, EN, JK)

17.12. Written examination (JH)

Poslední úprava: Hraníček Jakub, RNDr., Ph.D. (08.10.2024)

Literatura

Presentation from individual lectures are main literature sources for examination.

 

Extended information are avaible here.

Handbook of High-resolution Spectroscopy. Wiley 2011

Laser Chemistry. Spectroscopy, Dynamics and Applications. Wiley 2007

Surface Enhanced Raman Spectroscopy. Analytical, Bioanalytical and Life Science Application. Wiley 2010 

Modern Spectroscopy. 4th Ed. Wiley 2004

Poslední úprava: Hraníček Jakub, RNDr., Ph.D. (07.10.2024)

Požadavky ke zkoušce

a) Short oral presentation about the selected topic.

b) Written examination of the topics being taught.

Poslední úprava: Hraníček Jakub, RNDr., Ph.D. (07.10.2024)

Sylabus

1. Introduction to the Analytical Spectrometry (basic relations, analysis)

2. X-ray Spectrometry (principles, practical analysis)

3. Atomic Emission Spectrometry

4. Atomic Absorption Spectrometry

5. Atomic Fluorescence Spectrometry

6. Molecular Spectrometry in UV/VIS regions

7. Molecular Fluorescence

8. Infrared and Raman Spectrometry

9. Nuclear Magnetic Resonance

10. Other methods of Analytical Spectrometry

Poslední úprava: Hraníček Jakub, RNDr., Ph.D. (07.10.2024)

Výsledky učení

• Introduction to Analytical Spectrometry

  • The student explains the basic relationships and principles of analytical spectrometry.
  • The student clarifies the methods of analysis used in analytical spectrometry.

• X-ray Spectrometry

  • The student describes the principles of X-ray spectrometry.
  • The student applies X-ray spectrometry for the practical analysis of samples.

• Atomic Emission Spectrometry

  • The student explains the principles of atomic emission spectrometry.
  • The student applies atomic emission spectrometry for material analysis.

• Atomic Absorption Spectrometry

  • The student clarifies the basic principles of atomic absorption spectrometry.
  • The student determines the correct conditions for analysis using atomic absorption spectrometry.

• Atomic Fluorescence Spectrometry

  • The student distinguishes between absorption and fluorescence spectrometry.
  • The student applies atomic fluorescence spectrometry in analytical procedures.

• Molecular Spectrometry in UV/VIS Regions

  • The student describes the principles of molecular spectrometry in the UV/VIS region.
  • The student explains the relationship between light absorption and chemical structure.

• Molecular Fluorescence

  • The student explains the principles of molecular fluorescence.
  • The student applies fluorescence methods for molecular detection.

• Infrared and Raman Spectrometry

  • The student distinguishes between infrared and Raman spectrometry.
  • The student applies IR and Raman spectrometry in the analysis of chemical samples.

• Nuclear Magnetic Resonance

  • The student explains the principles of Nuclear Magnetic Resonance (NMR).
  • The student applies NMR spectrometry to determine chemical structures.

• Other Methods of Analytical Spectrometry

  • The student compares different methods of analytical spectrometry.
  • The student evaluates the suitability of various spectrometric methods for different types of analysis.

Poslední úprava: Hraníček Jakub, RNDr., Ph.D. (07.10.2024)