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X-ray Diffraction Study of Real Structure of Solids - NFPL029
Title: Rentgenové difrakční studium reálné struktury PL
Guaranteed by: Department of Condensed Matter Physics (32-KFKL)
Faculty: Faculty of Mathematics and Physics
Actual: from 2020
Semester: winter
E-Credits: 2
Hours per week, examination: winter s.:1/0, Ex [HT]
Capacity: unlimited
Min. number of students: unlimited
4EU+: no
Virtual mobility / capacity: no
State of the course: taught
Language: Czech, English
Teaching methods: full-time
Teaching methods: full-time
Guarantor: prof. RNDr. Radomír Kužel, CSc.
RNDr. Milan Dopita, Ph.D.
Classification: Physics > Solid State Physics
Annotation -
Last update: T_KFES (23.05.2001)
Kinematic theory of diffraction by real crystals. Study of lattice defects, size and shapes of crystallites, residual stresses, textures, lattice vibrations. Diffuse scattering. Small-angle scattering. X-ray topography.
Course completion requirements -
Last update: prof. RNDr. Radomír Kužel, CSc. (12.05.2022)

Oral exam from the content of the lecture

Literature - Czech
Last update: RNDr. Pavel Zakouřil, Ph.D. (05.08.2002)
  • V. Valvoda, M. Polcarová, P. Lukáč : Základy strukturní analýzy. Karolinum. Praha. 1992
  • I. Kraus : Úvod do strukturní rentgenografie. Academia. Praha 1985
  • I. Kraus., V.V. Trofimov : Rentgenová tenzometrie. Academia. Praha 1988. Quantitative Texture Analysis. ed. H.J. Bunge, C. Esling. DGM. Oberursel. 1982
  • Experimentální techniky v rentgenové a neutronové strukturní analýze. Krystalografická společnost. Praha 1994. ed. R. Kužel
  • Difrakcia na polykryštalických látkach.R & D. Print. Bratislava. 1994. red. L. Smrčok
  • dále vybrané články z časopisů

Syllabus -
Last update: T_KFES (26.05.2003)

1. Kinematic theory of diffraction by real crystals.

Krivoglaz theory, diffraction by ideal and real crystal, classification of lattice defects from the point of view of diffraction pattern, possibilities of their study.

2. Residual stresses.

Classification of stresses, description of stresses, stresses in thin films Stress measurement, triple-axis stresses.

3. Textures

General description of texture, pole figures, ODF, textures in thin films, residual stresses in textured samples, texture and physical properties

4. Line profile analysis

Correction of instrumental broadening, size-strain separation by different methods.

5. Study of lattice defects from line broadening

Dislocations and dislocation structures. Stacking faults.

6. Study of crystallite size, shape and distributions.

7. Study of lattice defects from change of diffracted intensities.

Description of displacement field, lattice parameter changes, static displacements, Debye-Waller factors

8. Diffuse scattering.

Thermal and structure diffuse scattering, geometrical and chemical disorder Huang scattering by point defects and their clusters

9. Scattering by precipitates and dislocation loops.

10. Defects in single crystals. X-ray topography.

11. Small-angle scattering.

 
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