SubjectsSubjects(version: 953)
Course, academic year 2023/2024
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Advaced Laboratory Training - MC240C25
Title: Pokročilé praktikum z laboratorní techniky
Czech title: Pokročilé praktikum z laboratorní techniky
Guaranteed by: Department of Inorganic Chemistry (31-240)
Faculty: Faculty of Science
Actual: from 2023
Semester: winter
E-Credits: 3
Examination process: winter s.:
Hours per week, examination: winter s.:0/5, C [DS]
Capacity: 8
Min. number of students: unlimited
4EU+: no
Virtual mobility / capacity: no
State of the course: not taught
Language: Czech
Additional information: https://dl2.cuni.cz/course/view.php?id=2050
Note: enabled for web enrollment
Guarantor: prof. RNDr. Petr Hermann, Dr.
Annotation -
The student labs are focused mostly on inert atmosphere techniques and on manipulations with air and temperature sensitive samples. The techniques: Schlenk apparatures (starting materials, reactions, filtration, distillation, preparation of samples for physico-chemical measurements); works with portable glovebox (set-up of glovebox before work, sample preparation); double vacuum-argon manifold and connectivities with Schlenk technique. Work with liquid gases and under low-temperature conditions. Using of septa.

The course is suitable for students of the second and third year of bachalor degree and for students of master degree.
Last update: Kubíček Vojtěch, doc. RNDr., Ph.D. (13.09.2016)
Literature -
  • Inorganic Syntheses, Book Series, Wiley, 1939 - 2012.
Last update: Hermann Petr, prof. RNDr., Dr. (08.08.2020)
Requirements to the exam -

Students are required to finish all preparations, to understand principles of the syntheses and methods and to write lab reports.

Last update: Kubíček Vojtěch, doc. RNDr., Ph.D. (26.10.2019)
Syllabus -

The student labs are focused mostly on inert atmosphere techniques and on manipulations with air and temperature sensitive samples.

The techniques: Schlenk apparatures (starting materials, reactions, filtration, distillation, preparation of samples for physico-chemical measurements); works with portable glovebox (set-up of glovebox before work, sample preparation); double vacuum-argon manifold and connectivities with Schlenk technique. Work with liquid gases and under low-temperature conditions. Using of septa.

The course is suitable for students of the second and third year of bachalor degree and for students of master degree.

Last update: Hermann Petr, prof. RNDr., Dr. (08.08.2020)
 
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