Subjects

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Advanced Inorganic Synthesis - Laboratory Exercise - MC240C21

Title:	Anorganické praktikum pro pokročilé
Guaranteed by:	Department of Inorganic Chemistry (31-240)
Faculty:	Faculty of Science
Actual:	from 2019
Semester:	winter
E-Credits:	12
Examination process:	winter s.:
Hours per week, examination:	winter s.:0/15, MC [DS]
Capacity:	unlimited
Min. number of students:	unlimited
4EU+:	no
Virtual mobility / capacity:	no
State of the course:	cancelled
Language:	Czech
Is provided by:	MC240C20
Note:	enabled for web enrollment

Guarantor:	prof. RNDr. Petr Štěpnička, Ph.D., DSc.
Teacher(s):	RNDr. Jiří Schulz, Ph.D.
Incompatibility :	MC240C20

Opinion survey results Examination dates Schedule

Annotation -

Last update: prof. RNDr. Petr Štěpnička, Ph.D., DSc. (06.12.2011)

This practical laboratory course is focused on the preparation and characterisation of inorganic compounds and materials in relation to courses of advanced inorganic and organometallic chemistry. Students learn special synthetic techniques (e.g., Schlenk techniques, handling of liquid gases and air-sensitive compounds, preparation at microscale, purification of by means of chromatographic methods and crystallisation). The compounds are characterised using appropriate methods (multinuclear NMR, UV-VIS, IR spectroscopies, mass spectrometry etc.). The laboratory course takes 15 days in winter semester and is designed for first year master degree students.

Literature -

Last update: prof. RNDr. Petr Štěpnička, Ph.D., DSc. (06.12.2011)

Any textbook of Advanced preparative inorganic chemistry and then literature relating to the individual syntheses.

Requirements to the exam -

Last update: prof. RNDr. Petr Štěpnička, Ph.D., DSc. (06.12.2011)

Credits are awarded when all the syntheses are completed, the compounds prepared duly characterised and the experimental work completely presented in laboratory notes.

Syllabus -

Last update: prof. RNDr. Petr Štěpnička, Ph.D., DSc. (06.12.2011)

During this course, students are expected to carry out several model preparations to cover fields mentioned in Annotation and to adequately characterise all compounds prepared.