SubjectsSubjects(version: 953)
Course, academic year 2023/2024
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Advanced Inorganic Synthesis - Laboratory Exercise - MC240C20
Title: Anorganické praktikum pro pokročilé
Czech title: Anorganické praktikum pro pokročilé
Guaranteed by: Department of Inorganic Chemistry (31-240)
Faculty: Faculty of Science
Actual: from 2019 to 2023
Semester: winter
E-Credits: 8
Examination process: winter s.:
Hours per week, examination: winter s.:0/15, MC [DS]
Capacity: unlimited
Min. number of students: unlimited
4EU+: no
Virtual mobility / capacity: no
State of the course: taught
Language: Czech
Note: enabled for web enrollment
Guarantor: RNDr. Jiří Schulz, Ph.D.
Teacher(s): RNDr. Jiří Schulz, Ph.D.
Is incompatible with: MC240C21, MC240P20E
Annotation -
This practical laboratory course is focused on the preparation and characterisation of inorganic compounds and materials in relation to courses of advanced inorganic and organometallic chemistry. Students learn special synthetic techniques (e.g., Schlenk techniques, handling of liquid gases and air-sensitive compounds, preparation at microscale, purification of by means of chromatographic methods and crystallisation). The compounds are characterised using appropriate methods (multinuclear NMR, UV-VIS, IR spectroscopies, mass spectrometry etc.). The laboratory course takes 15 days in winter semester and is designed for first year master degree students.
Last update: Kubíček Vojtěch, doc. RNDr., Ph.D. (22.04.2015)
Literature -

Any textbook of Advanced preparative inorganic chemistry and then literature relating to the individual syntheses.

Last update: Kubíček Vojtěch, doc. RNDr., Ph.D. (22.04.2015)
Requirements to the exam -

Credits are awarded when all the syntheses are completed, the compounds prepared duly characterised and the experimental work completely presented in laboratory notes.

Last update: Kubíček Vojtěch, doc. RNDr., Ph.D. (22.04.2015)
Syllabus -

During this course, students are expected to carry out several model preparations to cover fields mentioned in Annotation and to adequately characterise all compounds prepared.

Last update: Kubíček Vojtěch, doc. RNDr., Ph.D. (22.04.2015)
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