SubjectsSubjects(version: 953)
Course, academic year 2023/2024
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Instrumental Methods in Inorganic Chemistry - MC240C15
Title: Instrumental Methods in Inorganic Chemistry
Czech title: Praktikum z fyzikálních metod studia anorganických látek
Guaranteed by: Department of Inorganic Chemistry (31-240)
Faculty: Faculty of Science
Actual: from 2022 to 2023
Semester: summer
E-Credits: 9
Examination process: summer s.:
Hours per week, examination: summer s.:0/6, MC [HT]
Capacity: unlimited
Min. number of students: unlimited
4EU+: no
Virtual mobility / capacity: no
State of the course: taught
Language: English
Note: enabled for web enrollment
Guarantor: doc. RNDr. Róbert Gyepes, Dr., Ph.D.
Teacher(s): RNDr. Ivana Císařová, CSc.
doc. RNDr. Róbert Gyepes, Dr., Ph.D.
doc. RNDr. David Havlíček, CSc.
prof. RNDr. Petr Hermann, Dr.
prof. RNDr. Jana Kalbáčová Vejpravová, Ph.D.
doc. RNDr. Vojtěch Kubíček, Ph.D.
RNDr. Alan Liška, Ph.D.
prof. RNDr. Jiří Mosinger, Ph.D.
prof. RNDr. Ivan Němec, Ph.D.
RNDr. Jiří Schulz, Ph.D.
Class: Sestava HPLC-MS
Původní předmět
Co-requisite : MC240P15
Incompatibility : MC240C26
Is incompatible with: MC240C26
Annotation -
The laboratory course is aimed at providing practical experiences and a brief survey of principles and
applications of physical methods used in inorganic chemistry.

The course is designed for Master and PhD students.
Last update: Kubíček Vojtěch, doc. RNDr., Ph.D. (06.05.2021)
Literature -

Luerature is recommended by supervisors of selected exercises.

Last update: Kubíček Vojtěch, doc. RNDr., Ph.D. (06.05.2021)
Requirements to the exam -

Protocols of individual excercises are to be submitted to their leaders for inspection always within one week upon completing any excersize.

After the completion of all excersises prescribed, their acepted and signed protocols have to be delivered to the course supervisor within three weeks.

The classification of individual protocols will reflect not only the protocol quality, but also their timely submission.

 

In the case of timely protocol submission to the course supervisor, the final classification is calculated as the average of classifications achieved within all individual excerises.

In case of later submission without proving a serious reason, the final classification is worsened by one degree with respect to the classification for a timely submission.

Should the delay in submitting the protocols exceed two months for no serious reason, the final classification obtained from averaging the individual classifications will be worsened by two degrees.

Last update: Kubíček Vojtěch, doc. RNDr., Ph.D. (06.05.2021)
Syllabus -

This practical course consists of nine compulsory exercises and four further excersizes to be selected from a group.

Compulsory exercises:

1.    Quantitative analysis using X-ray power diffration
2.    Structure analysis using single-crystal X-ray diffraction
3.    Vibrational spectroscopy I. (IR + Raman)
4.    NMR spectroscopy
5.    Potentiometry
6.    Electronic spectroscopy

Selectable exercises:

Each student chooses four additional exercises from the below list. Venue dates are set individually after discussing with the exercise heads within one week following the introductory instruction.

7. High-temperature powder X-ray diffraction
8. Vibrational spectroscopy II. (IR + Raman microspectroscopy)
9. Magnetochemistry
10. Study of phase transitions by IR/Raman spectroscopy
11. Thermal capacity of solid-state compounds – thermal dependence
12. Magnetic phase transitions
13. EPR spectroscopy
14. Fluorimetry
15. Application of quantum-chemical methods for studying physical and chemical properties
16. Voltammetric methods
17. Hyperthermy of magnetic nanoparticles
18. Basic ferromagnet characteristics
19. High performance liquid chromatography with mass detection
20. Mossbauer spectroscopy

Last update: Němec Ivan, prof. RNDr., Ph.D. (22.02.2024)
 
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