Subjects

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Selected Methods of Laboratory Technique - GF227

Title:	Vybrané metody laboratorní techniky
Guaranteed by:	Department of Organic And Bioorganic Chemistry (16-16120)
Faculty:	Faculty of Pharmacy in Hradec Králové
Actual:	from 2024
Semester:	summer
Points:	0
E-Credits:	1
Examination process:	summer s.:
Hours per week, examination:	summer s.:0/28, C [HS]
Capacity:	unknown / unknown (24)
Min. number of students:	unlimited
4EU+:	no
Virtual mobility / capacity:	no
Key competences:
State of the course:	not taught
Language:	Czech
Teaching methods:	full-time
Teaching methods:	full-time
Level:
Explanation:	(F 2.r.)
Note:	deregister from the credit exam date if a requisite was not fulfilled course can be enrolled in outside the study plan enabled for web enrollment

Guarantor:	PharmDr. Petr Matouš, Ph.D.
Pre-requisite :	GF124, GF285
Interchangeability :	GF400
Is interchangeable with:	GF400

Examination dates Schedule

Annotation -

Optional subject for 2nd year students. Practical classes succeeding to Chemical Laboratory Technique, which extend its basic laboratory technique to a more complex level.

Last update: Matouš Petr, PharmDr., Ph.D. (14.02.2024)

Course completion requirements -

Requirements for gaining the credit in subject „Selected methods of Laboratory Technique“:

100% attendance at practical classes
Completed protocols from all exercises

Last update: Matouš Petr, PharmDr., Ph.D. (14.02.2024)

Literature -

Obligatory:

. . In Hrabálek, Alexandr. Chemická laboratorní technika pro farmaceuty . Praha: Univerzita Karlova, Nakladatelství Karolinum, 2016, s. -. ISBN 978-80-246-3515-6..

Last update: prepocet_literatura.php (19.09.2024)

Syllabus -

Syllabus:

Simple distillation, fractional distillation, distillation under reduced pressure, distillation under inert gas, rotary vacuum evaporator: principles and carrying out.
Chromatography: principles & techniques, column chromatography – separation of four-component mixture, thin layer chromatography – separation of mixtures, methods of detection.
Monitoring and comparison of conversion rate of reaction carried out: at room temperature, under reflux, in microwave reactor. Identification of product.
Reactions carried out under inert gas: types of reactions, principles & techniques. Identification of product.

Last update: Matouš Petr, PharmDr., Ph.D. (14.02.2024)

Entry requirements -

Subject Selected Methods of Laboratory Technique can be registered after passing subject General and Inorganic Chemistry (GF124) and Organic Chemistry I (GF285).

Last update: Matouš Petr, PharmDr., Ph.D. (14.02.2024)