Subjects

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Chemical Laboratory Technique - GAF369

Title:	Chemical Laboratory Technique
Guaranteed by:	Department of Organic And Bioorganic Chemistry (16-16120)
Faculty:	Faculty of Pharmacy in Hradec Králové
Actual:	from 2023
Semester:	winter
Points:	0
E-Credits:	2
Examination process:	winter s.:
Hours per week, examination:	winter s.:0/56, C [HS]
Capacity:	unknown / unlimited (unknown)
Min. number of students:	unlimited
4EU+:	no
Virtual mobility / capacity:	no
Key competences:
State of the course:	taught
Language:	English
Teaching methods:	full-time
Teaching methods:	full-time
Level:
Note:	deregister from the credit exam date if a requisite was not fulfilled course can be enrolled in outside the study plan enabled for web enrollment

Guarantor:	doc. PharmDr. Mgr. Martin Krátký, Ph.D.
Comes under:	2.ročník 2023/24 Pharmacy (EN19)
Incompatibility :	GAF130
Pre-requisite :	GAF124, GAF285
Interchangeability :	GAF130
Is co-requisite for:	GAF035
Is interchangeable with:	GAF130

Examination dates WS schedule

Annotation -

Last update: doc. PharmDr. Mgr. Martin Krátký, Ph.D. (21.09.2023)

The subject Chemical Laboratory Technique provides introduction to basic and advanced methods employed in a chemistry lab. Students will gain the knowledge about the function and equipment of a chemistry lab and will perform modern methods of synthesis, separation, purification and characterization of the resultant products.

Course completion requirements -

Last update: doc. PharmDr. Mgr. Martin Krátký, Ph.D. (21.09.2023)

Credit Requirements:

•attendance at all practical classes

•completed protocols

•passing credit test (60 % of a total score is necessary)

•in the case of unfavorable epidemic situation wil be all details of accomplishment announced

Literature -

Last update: doc. PharmDr. Mgr. Martin Krátký, Ph.D. (21.09.2023)

Obligatory:

Palát, Karel, Macháček, Miloš. Laboratory manual for general and inorganic chemistry : určeno pro posl. farmaceut. fakulty Univ. Karlovy. Praha: Karolinum, 1993, 109 s. ISBN 80-7066-751-6.

Syllabus -

Last update: doc. PharmDr. Mgr. Martin Krátký, Ph.D. (21.09.2023)

Syllabus:

Safety instructions
First aid in a chemistry lab
Introduction to chemistry lab
Laboratory glassware
Heating of the reaction mixtures - possible methods
Stirring of the reaction mixtures - possible methods
Methods of cooling of the reaction mixtures
Purification of solid chemicals - crystallization
Purification of liquid chemicals - distillation
Isolation of products
Extraction
Liquid and solid chemicals drying
Gases preparation and handling
Characterization of chemicals
Spectral methods in organic synthesis
Thin-layer chromatography

Entry requirements -

Last update: doc. PharmDr. Mgr. Martin Krátký, Ph.D. (21.09.2023)

Subject Chemical Laboratory Technique can be registered after passing subject General and Inorganic Chemistry (GAF124) and Organic Chemistry I (GAF285).