Selected Methods of Laboratory Technique - GAF227
Title: Selected Methods of Laboratory Technique
Guaranteed by: Department of Organic And Bioorganic Chemistry (16-16120)
Faculty: Faculty of Pharmacy in Hradec Králové
Actual: from 2024
Semester: summer
Points: 0
E-Credits: 1
Examination process: summer s.:
Hours per week, examination: summer s.:0/28, C [HS]
Capacity: unknown / unknown (24)
Min. number of students: unlimited
4EU+: no
Virtual mobility / capacity: no
Key competences:  
State of the course: not taught
Language: English
Teaching methods: full-time
Level:  
Explanation: (F 2.r.)
Note: deregister from the credit exam date if a requisite was not fulfilled
course can be enrolled in outside the study plan
enabled for web enrollment
Guarantor: doc. Dr. Russell Richard Anthony Kitson
Pre-requisite : GAF124, GAF285
Is interchangeable with: GAF400
Examination dates   Schedule   
Annotation -
Optional subject for 2nd year students. Practical classes succeeding to Chemical Laboratory Technique, which extend its basic laboratory technique to a more complex level.
Last update: Kitson Russell Richard Anthony, doc. Dr. (15.02.2024)
Course completion requirements -

Requirements for gaining the credit in subject „Selected methods of Laboratory Technique“:

 

1)         100% attendance at practical classes

2)         completed protocols from all exercises

Last update: Kitson Russell Richard Anthony, doc. Dr. (15.02.2024)
Literature -

Obligatory:

  • . . In Palát, Karel, Macháček, Miloš. Laboratory manual for general and inorganic chemistry : určeno pro posl. farmaceut. fakulty Univ. Karlovy . Praha: Karolinum, 1993, s. -. ISBN 80-7066-751-6..

Recommended:

  • . . In Williams and Fleming. Spectral Methods in Organic Chemistry . : , , s. -. ISBN ..

Last update: prepocet_literatura.php (19.09.2024)
Syllabus -

Syllabus:

  1. Simple distillation, fractional distillation, distillation under reduced pressure, distillation under inert gas, rotary vacuum evaporator: principles and carrying out.

  2. Chromatography: principles & techniques, column chromatography – separation of four-component mixture, thin layer chromatography – separation of mixtures, methods of detection.

  3. Monitoring and comparison of conversion rate of reaction carried out: at room temperature, under reflux, in microwave reactor. Identification of product. Reactions carried out under inert gas

  4. Spectroscopy and structure elucidation

Last update: Kitson Russell Richard Anthony, doc. Dr. (15.02.2024)
Entry requirements -

Subject Selected Methods of Laboratory Technique can be registered after passing subject General and Inorganic Chemistry (GAF124) and Organic Chemistry I (GAF285).

 

Last update: Kitson Russell Richard Anthony, doc. Dr. (15.02.2024)