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Course, academic year 2023/2024
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Selected Methods of Laboratory Technique - GF227
Title: Vybrané metody laboratorní techniky
Guaranteed by: Department of Organic And Bioorganic Chemistry (16-16120)
Faculty: Faculty of Pharmacy in Hradec Králové
Actual: from 2022
Semester: summer
Points: 0
E-Credits: 1
Examination process: summer s.:
Hours per week, examination: summer s.:0/28, C [HS]
Capacity: unknown / 50 (24)
Min. number of students: unlimited
4EU+: no
Virtual mobility / capacity: no
Key competences:  
State of the course: taught
Language: Czech
Teaching methods: full-time
Teaching methods: full-time
Level:  
Explanation: (F 2.r.)
Note: deregister from the credit exam date if a requisite was not fulfilled
course can be enrolled in outside the study plan
enabled for web enrollment
Guarantor: PharmDr. Petr Matouš, Ph.D.
Comes under: 2.ročník 2023/24 Farmacie
Pre-requisite : GF124, GF285
Annotation -
Last update: PharmDr. Petr Matouš, Ph.D. (14.02.2024)
Optional subject for 2nd year students. Practical classes succeeding to Chemical Laboratory Technique, which extend its basic laboratory technique to a more complex level.
Course completion requirements -
Last update: PharmDr. Petr Matouš, Ph.D. (14.02.2024)

Requirements for gaining the credit in subject „Selected methods of Laboratory Technique“: 

  1. 100% attendance at practical classes
  2. Completed protocols from all exercises
Literature -
Last update: PharmDr. Petr Matouš, Ph.D. (14.02.2024)

Obligatory:

  • . . In Hrabálek, Alexandr. Chemická laboratorní technika pro farmaceuty . Praha: Univerzita Karlova, Nakladatelství Karolinum, 2016, s. -. ISBN 978-80-246-3515-6..
Syllabus -
Last update: PharmDr. Petr Matouš, Ph.D. (14.02.2024)

Syllabus:

  1. Simple distillation, fractional distillation, distillation under reduced pressure, distillation under inert gas, rotary vacuum evaporator: principles and carrying out.

  2. Chromatography: principles & techniques, column chromatography – separation of four-component mixture, thin layer chromatography – separation of mixtures, methods of detection.

  3. Monitoring and comparison of conversion rate of reaction carried out: at room temperature, under reflux, in microwave reactor. Identification of product.

  4. Reactions carried out under inert gas: types of reactions, principles & techniques. Identification of product.
Entry requirements -
Last update: PharmDr. Petr Matouš, Ph.D. (14.02.2024)

Subject Selected Methods of Laboratory Technique can be registered after passing subject General and Inorganic Chemistry (GF124) and Organic Chemistry I (GF285).
 
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