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Course, academic year 2023/2024
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Organic chemistry - Laboratory course B - MC270C98N
Title: Organické praktikum B
Czech title: Organické praktikum B
Guaranteed by: Department of Organic Chemistry (31-270)
Faculty: Faculty of Science
Actual: from 2022
Semester: both
E-Credits: 4
Hours per week, examination: 0/2, C [TS]
Capacity: unlimited
Min. number of students: 3
4EU+: no
Virtual mobility / capacity: no
State of the course: cancelled
Language: Czech, English
Explanation: Začátek cvičení je před laboratoří č. 145 na katedře organické chemie.Skripta Veselý J. ; Machara A. : Příručka laboratorní organické chemie, UK 2020Povinně s sebou : laboratorní plášť, ochranné brýle a pevná obuv
Additional information: http://web.natur.cuni.cz/~lorenc/
Note: priority enrollment if the course is part of the study plan
you can enroll for the course in winter and in summer semester
Guarantor: Ing. Miroslav Lorenc
Is incompatible with: MC270C92
Is interchangeable with: MC270C62N, MC270C26, MC270C57U
Opinion survey results   Examination dates   Schedule   
Annotation -
Last update: Ing. Miroslav Lorenc (07.06.2018)
The basic practice of organic chemistry have the task to teach students the basics of laboratory techniques
and methodology of work in the organic laboratory.
Synthetic tasks are chosen so that the students are acquainted with basic chemical operations, and to obtain information
on the preparation and properties of organic compounds.
Students thus have to supplement the theoretical knowledge from the lectures of organic chemistry.

Filling the practice :
1. Basic operations in organic laboratory: procedures of isolation organic substances; clearing
operations; monitoring the progress of reactions; chromatographic methods
2. Work safety and first aid in the organic laboratory.
3. Laboratory technique : the construction of the apparatus for chemical reaction; mixing;
heating; cooling; work under reduced pressure in an inert atmosphere, and if protected
from humidity
4. Cleaning and isolation procedures : filtration; washing; extraction and roztřepávání; drtiny
of solids and liquids; crystallization
5. Distillation : simple distillation; distillation under reduced pressure; mastering the work
with the rotary vacuum evaporator
6. Thin layer chromatography .
7. The leadership of the working of the protocol.
Literature - Czech
Last update: Ing. Miroslav Lorenc (16.09.2020)

Veselý J. ; Machara A. : Příručka laboratorní organické chemie, skriptum UK , Praha 2020

Trnka a kol.: Praktikum z organické chemie
Kvíčala J. : Laboratorní technika organické chemie, skriptum VŠCHT, Praha 1996

Requirements to the exam -
Last update: Ing. Miroslav Lorenc (07.06.2018)

The Student must write on a 60 % final test.

The Student must prepare according to the laboratory regulations 8 compounds and surrender them, together with the protocols.

Syllabus -
Last update: Ing. Miroslav Lorenc (07.06.2018)

 The Student gets a list of organic compounds which has a prepare, at the beginning of the practice.

Entry requirements -
Last update: Ing. Miroslav Lorenc (07.06.2018)

Required a good foundation in general science basis covering the fundamentals of high school mathematics, physics and general and organic chemistry.

 
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