Organic chemistry - Laboratory course B - MC270C98N
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Last update: Ing. Miroslav Lorenc (07.06.2018)
and methodology of work in the organic laboratory. Synthetic tasks are chosen so that the students are acquainted with basic chemical operations, and to obtain information on the preparation and properties of organic compounds. Students thus have to supplement the theoretical knowledge from the lectures of organic chemistry. Filling the practice : 1. Basic operations in organic laboratory: procedures of isolation organic substances; clearing operations; monitoring the progress of reactions; chromatographic methods 2. Work safety and first aid in the organic laboratory. 3. Laboratory technique : the construction of the apparatus for chemical reaction; mixing; heating; cooling; work under reduced pressure in an inert atmosphere, and if protected from humidity 4. Cleaning and isolation procedures : filtration; washing; extraction and roztřepávání; drtiny of solids and liquids; crystallization 5. Distillation : simple distillation; distillation under reduced pressure; mastering the work with the rotary vacuum evaporator 6. Thin layer chromatography . 7. The leadership of the working of the protocol. |
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Last update: Ing. Miroslav Lorenc (16.09.2020)
Veselý J. ; Machara A. : Příručka laboratorní organické chemie, skriptum UK , Praha 2020 Trnka a kol.: Praktikum z organické chemie |
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Last update: Ing. Miroslav Lorenc (07.06.2018)
The Student must write on a 60 % final test. The Student must prepare according to the laboratory regulations 8 compounds and surrender them, together with the protocols. |
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Last update: Ing. Miroslav Lorenc (07.06.2018)
The Student gets a list of organic compounds which has a prepare, at the beginning of the practice. |
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Last update: Ing. Miroslav Lorenc (07.06.2018)
Required a good foundation in general science basis covering the fundamentals of high school mathematics, physics and general and organic chemistry. |